| Schedule 2033 |
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| Description:
NAWQA Schedule 2003 plus 20 additional compounds |
|
| Owner:
NAWQA |
|
| Analyzing
Laboratory(s): |
|
| USGS -
National Water Quality Laboratory, Denver, CO |
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|
| Analyte |
|
CAS Number |
RL |
Unit |
|
| 1-Naphthol |
|
90-15-3 |
0.0882 |
ug/L |
|
| 2-Chloro-2,6-diethylacetanilide |
6967-29-9 |
0.005 |
ug/L |
|
| 2-Ethyl-6-methylaniline |
24549-06-2 |
0.0045 |
ug/L |
|
| 3,4-Dichloroaniline |
95-76-1 |
0.0045 |
ug/L |
|
| 3,5-Dichloroaniline |
626-43-7 |
0.0043 |
ug/L |
|
| 4-Chloro-2-methylphenol |
1570-64-5 |
0.0056 |
ug/L |
|
| Acetochlor |
|
34256-82-1 |
0.006 |
ug/L |
|
| Alachlor |
|
15972-60-8 |
0.005 |
ug/L |
|
| 2,6-Diethylaniline |
579-66-8 |
0.006 |
ug/L |
|
| Atrazine |
|
1912-24-9 |
0.007 |
ug/L |
|
| Azinphos-methyl |
86-50-0 |
0.05 |
ug/L |
|
| Azinphos-methyl-oxon |
961-22-8 |
0.07 |
ug/L |
|
| Benfluralin |
|
1861-40-1 |
0.01 |
ug/L |
|
| Carbaryl |
|
63-25-2 |
0.041 |
ug/L |
|
| Carbofuran |
|
1563-66-2 |
0.02 |
ug/L |
|
| Chlorpyrifos |
2921-88-2 |
0.005 |
ug/L |
|
| Chlorpyrofos, oxygen analog |
5598-15-2 |
0.0562 |
ug/L |
|
| cis-Permethrin |
54774-45-7 |
0.006 |
ug/L |
|
| cis-Propiconazole |
60207-90-1 |
0.008 |
ug/L |
|
| Cyanazine |
|
21725-46-2 |
0.018 |
ug/L |
|
| Cyfluthrin |
|
68359-37-5 |
0.0267 |
ug/L |
|
| Cypermethrin |
52315-07-8 |
0.0086 |
ug/L |
|
| Dacthal |
|
1861-32-1 |
0.003 |
ug/L |
|
| 2-Chloro-4-isopropylamino-6-amino-s-triazine {CIAT} |
6190-65-4 |
0.006 |
ug/L |
|
| Diazinon |
|
333-41-5 |
0.005 |
ug/L |
|
| Diazinon, oxygen analog |
962-58-3 |
0.006 |
ug/L |
|
| Diazinon-d10 |
100155-47-3 |
|
pct |
|
| Dichlorvos |
|
62-73-7 |
0.0118 |
ug/L |
|
| Dicrotophos |
141-66-2 |
0.0843 |
ug/L |
|
| Dieldrin |
|
60-57-1 |
0.009 |
ug/L |
|
| Dimethoate |
60-51-5 |
0.0061 |
ug/L |
|
| Disulfoton |
|
298-04-4 |
0.021 |
ug/L |
|
| Disulfoton sulfone |
6/5/2497 |
0.0059 |
ug/L |
|
| alpha-Endosulfan |
959-98-8 |
0.0047 |
ug/L |
|
| Endosulfan sulfate |
1031-07-8 |
0.0138 |
ug/L |
|
| EPTC |
|
759-94-4 |
0.004 |
ug/L |
|
| Ethion |
|
563-12-2 |
0.004 |
ug/L |
|
| Ethion monoxon |
17356-42-2 |
0.002 |
ug/L |
|
| Ethoprophos |
13194-48-4 |
0.005 |
ug/L |
|
| Fenamiphos |
22224-92-6 |
0.029 |
ug/L |
|
| Fenamiphos sulfone |
31972-44-8 |
0.0491 |
ug/L |
|
| Fenamiphos sulfoxide |
31972-43-7 |
0.0387 |
ug/L |
|
| Desulfinylfipronil amide |
|
0.029 |
ug/L |
|
| Fipronil sulfide |
120067-83-6 |
0.013 |
ug/L |
|
| Fipronil sulfone |
120068-36-2 |
0.024 |
ug/L |
|
| Desulfinylfipronil |
|
0.012 |
ug/L |
|
| Fipronil |
|
120068-37-3 |
0.016 |
ug/L |
|
| Fonofos |
|
944-22-9 |
0.003 |
ug/L |
|
| alpha-HCH-d6 |
86194-41-4 |
|
pct |
|
| Hexazinone |
51235-04-2 |
0.0129 |
ug/L |
|
| Iprodione |
|
36734-19-7 |
0.538 |
ug/L |
|
| Isofenphos |
|
25311-71-1 |
0.0034 |
ug/L |
|
| lambda-Cyhalothrin |
91465-08-6 |
0.0089 |
ug/L |
|
| Malaoxon |
|
1634-78-2 |
0.0298 |
ug/L |
|
| Malathion |
|
121-75-5 |
0.027 |
ug/L |
|
| Metalaxyl |
|
57837-19-1 |
0.0051 |
ug/L |
|
| Methidathion |
950-37-8 |
0.0058 |
ug/L |
|
| Parathion-methyl |
298-00-0 |
0.015 |
ug/L |
|
| Metolachlor |
51218-45-2 |
0.006 |
ug/L |
|
| Metribuzin |
|
21087-64-9 |
0.006 |
ug/L |
|
| Molinate |
|
2212-67-1 |
0.003 |
ug/L |
|
| Myclobutanil |
88671-89-0 |
0.008 |
ug/L |
|
| Oxyfluorfen |
42874-03-3 |
0.0073 |
ug/L |
|
| Paraoxon-methyl |
950-35-6 |
0.0299 |
ug/L |
|
| Pendimethalin |
40487-42-1 |
0.022 |
ug/L |
|
| Phorate |
|
298-02-2 |
0.011 |
ug/L |
|
| Phorate oxygen analog |
2600-69-3 |
0.1048 |
ug/L |
|
| Phosmet |
|
732-11-6 |
0.0079 |
ug/L |
|
| Phosmet oxon |
3735-33-9 |
0.0511 |
ug/L |
|
| Prometon |
|
1610-18-0 |
0.01 |
ug/L |
|
| Prometryn |
|
7287-19-6 |
0.0054 |
ug/L |
|
| Propyzamide |
23950-58-5 |
0.004 |
ug/L |
|
| Propanil |
|
709-98-8 |
0.011 |
ug/L |
|
| Propargite |
|
2312-35-8 |
0.023 |
ug/L |
|
| Sample volume |
|
mL |
|
| Set number |
|
no. |
|
| Simazine |
|
122-34-9 |
0.005 |
ug/L |
|
| Tebuconazole |
107534-96-3 |
0.0136 |
ug/L |
|
| Tebuthiuron |
34014-18-1 |
0.016 |
ug/L |
|
| Tefluthrin |
|
79538-32-2 |
0.0077 |
ug/L |
|
| Terbufos |
|
13071-79-9 |
0.017 |
ug/L |
|
| Terbufos oxygen analog sulfone |
56070-15-6 |
0.0676 |
ug/L |
|
| Terbuthylazine |
5915-41-3 |
0.0102 |
ug/L |
|
| Thiobencarb |
28249-77-6 |
0.01 |
ug/L |
|
| trans-Propiconazole |
60207-90-1 |
0.0133 |
ug/L |
|
| Tribufos |
|
78-48-8 |
0.0044 |
ug/L |
|
| Trifluralin |
|
1582-09-8 |
0.009 |
ug/L |
|
|
| Container
Requirements |
|
| Quantity |
Bottle |
|
| 1 |
1L GCC - This schedule consumes the
entire container. |
|
|
Description: |
|
|
Treatment and Preservation: 1L
125mL or 60mL (see schedule for size) Glass amber bottle baked at 450 deg C
by laboratory - SOME GCCs should be filtered CHECK METHOD REFERENCE OR EMAIL
LABHELP@USGS.GOV FOR FILTERING REQUIREMENTS? DO NOT RINSE BOTTLE. Do not fill
bottle beyond shoulder. reagents must be added to the sample at the NWQL
before analyses. Chill sample and maintain at 4 deg C. ship immediately. |
| References |
|
|
| 1. OFR 95-181 (original method) |
|
| Zaugg,
S.D., Sandstrom, M.W., Smith, S.G., and Fehlberg, K.M., 1995, Methods of
analysis by the U.S. Geological Survey National Water Quality
Laboratory--Determination of pesticides in water by C-18 solid-phase
extraction and capillary-column gas chromatography/mass spectrometry with
selected-ion monitoring: U.S. Geological Survey Open-File Report 95-181, 60
p. |
|
| Method ID:
O-1126-95 |
|
|
| 2.
Journal of AOAC Intl, v. 79, no. 4, p. 962-966 (Acetochlor) |
|
| Lindley,
C.E., Stewart, J.T., and Sandstrom, M.W., 1996, Determination of low
concentrations of acetochlor in water by automated solid-phase extraction and
gas chromatography with mass selective detection: Journal of AOAC
International, v. 79, no. 4, p. 962-966. |
|
|
| 3. OFR 02-462 (fipronil and
degradates) |
|
| Madsen,
J.E., Sandstrom, M.W., and Zaugg, S.D., 2003, Methods of analysis by the U.S.
Geological Survey National Water Quality Laboratory---A method supplement for
the determination of fipronil and degradates in water by gas
chromatography/mass spectrometry: U.S. Geological Survey Open-File Report
02-462, 11 p. |
|
| Method ID:
O-1126-02 |
|
|
| 4. WRIR 01-4098 |
|
| Sandstrom,
M.W., Stroppel, M.E., Foreman, W.T., and Schroeder, M.P., 2001, Methods of
analysis by the U.S. Geological Survey National Water Quality
Laboratory--Determination of moderate-use pesticides and selected degradates
in water by C-18 solid-phase extraction and gas chromatography/mass
spectrometry: U.S. Geological Survey Water-Resources Investigations Report
01-4098, 70 p. |
|
| Method ID:
O-2002-01 |
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